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Analysis of the Toad Poison Bufadienolides by Rod-Thin-Layer Chromatography with Flame Ionization Detector
http://hdl.handle.net/10487/1280
http://hdl.handle.net/10487/128079060f71-adf8-47fa-915b-a24d74f9a8f2
| 名前 / ファイル | ライセンス | アクション |
|---|---|---|
kana-1-6-0007.pdf (1.6 MB)
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| Item type | 紀要論文 / Departmental Bulletin Paper(1) | |||||
|---|---|---|---|---|---|---|
| 公開日 | 2009-02-23 | |||||
| タイトル | ||||||
| タイトル | Analysis of the Toad Poison Bufadienolides by Rod-Thin-Layer Chromatography with Flame Ionization Detector | |||||
| 言語 | ||||||
| 言語 | eng | |||||
| キーワード | ||||||
| 主題Scheme | Other | |||||
| 主題 | Rod-Thin-Layer Chromatography | |||||
| キーワード | ||||||
| 主題Scheme | Other | |||||
| 主題 | IATROSCAN | |||||
| キーワード | ||||||
| 主題Scheme | Other | |||||
| 主題 | Bufadienolides | |||||
| キーワード | ||||||
| 主題Scheme | Other | |||||
| 主題 | Ch'an Su | |||||
| キーワード | ||||||
| 主題Scheme | Other | |||||
| 主題 | Reactivity of Cinobufagin | |||||
| 資源タイプ | ||||||
| 資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
| 資源タイプ | departmental bulletin paper | |||||
| 著者 |
Kamano, Yoshiaki
× Kamano, Yoshiaki× 釜野, 徳明× Yamashita, Ayano× 山下, 文乃× Nogawa, Toshihiko× 野川, 俊彦× Takeuchi, Hiroaki× Kohyama, Koichi× Pettit, George R. |
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| 抄録 | ||||||
| 内容記述タイプ | Abstract | |||||
| 内容記述 | Analysis of the toad poison bufadienolides using the rod-thin-layer chromatography (Rod-TLC) with FID was undertaken. By the use of n-hexane/CH_2Cl_2/MeOH(11 : 8 : 1) as a developing solvent system, an effective separation of the eight bufadienolides-cinobufagin, resibufogenin, bufalin, bufotalin, desacetyl-cinobufagin, desacetyl-bufotalin, gamabufotalin and 3-oxo-cinobufagin-was obtained. Also, the reactivities of cinobufagin in oxidation and hydrolysis by using reaction mixture were checked by Rod-TLC. The contents of three major bufadienolides-resibufogenin, cinobufagin and bufalin-in the two kinds of Ch'an Su (the so-called "disk-like Ch'an Su" and "thin-plate Ch'an Su") were analyzed by the use of Rod-TLC (IATROSCAN). | |||||
| 書誌情報 |
年報 巻 '99, p. 29-38, 発行日 2000-03 |
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| 書誌レコードID | ||||||
| 収録物識別子タイプ | NCID | |||||
| 収録物識別子 | AA11822302 | |||||
| 著者版フラグ | ||||||
| 出版タイプ | VoR | |||||
| 出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
| 出版者 | ||||||
| 出版者 | 神奈川大学 | |||||
