@article{oai:kanagawa-u.repo.nii.ac.jp:00007379,
 author = {Kamano, Yoshiaki and 釜野, 徳明 and Yamashita, Ayano and 山下, 文乃 and Nogawa, Toshihiko and 野川, 俊彦 and Takeuchi, Hiroaki and Kohyama, Koichi and Pettit, George R.},
 journal = {年報},
 month = {Mar},
 note = {Analysis of the toad poison bufadienolides using the rod-thin-layer chromatography (Rod-TLC) with FID was undertaken. By the use of n-hexane/CH_2Cl_2/MeOH(11 : 8 : 1) as a developing solvent system, an effective separation of the eight bufadienolides-cinobufagin, resibufogenin, bufalin, bufotalin, desacetyl-cinobufagin, desacetyl-bufotalin, gamabufotalin and 3-oxo-cinobufagin-was obtained. Also, the reactivities of cinobufagin in oxidation and hydrolysis by using reaction mixture were checked by Rod-TLC. The contents of three major bufadienolides-resibufogenin, cinobufagin and bufalin-in the two kinds of Ch'an Su (the so-called "disk-like Ch'an Su" and "thin-plate Ch'an Su") were analyzed by the use of Rod-TLC (IATROSCAN).},
 pages = {29--38},
 title = {Analysis of the Toad Poison Bufadienolides by Rod-Thin-Layer Chromatography with Flame Ionization Detector},
 volume = {'99},
 year = {2000}
}